Institut de Chimie Moléculaire et des Matériaux d'Orsay

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Model

 

Thermofisher Scientific K-Alpha

Device

Electron analyzer and detector

  • Double focus hemispherical analyzer (180°)
  • ‘’Take off angle’’: 0°
  • Transition energy from 1 to 400 eV
  • Minimum step 3 meV
  • Acceptance angle 60 ° (+/- 30 °)
  • Detector MCP 128 channels

Monochromatized and micro-focused X source

  • Aluminum anode (Al Kα = 1486,7 eV)
  • Spot size from 30 to 400 μm
  • Working power: 72 W
  • Analyzer / X Ray angle: 56°

Combined low energy electron / ion scattering source for charge neutralization

  • ‘’Dual Beam’’ source type
  • Electron Energy typically from 0 to 5 eV
  • Electron Beam Current typically 250 μA
  • Ion Energy typically 20 eV
  • Ion Current typically 20 nA

Ion gun for depth profiles and sample cleaning

  • Energy range: 100 eV to 4 KeV
  • Maximum ion current : > 4 μA
  • Spot size: 200 μm to 2.5 μA and 4 KeV
  • Gas used: Ar

Spectrum processing software

Samples that can be analyzed

  • bulk
  • films
  • powders

Please note: sulfides, iodides and fluorides, especially in the form of powders, are excluded because they may pollute the analysis chamber.

You are requested to keep the samples you bring for analysis clean. The surfaces must not come into contact with the skin or the walls of the boxes in which the samples are stored.

 

Link to the XPS database maintained by this service:

http://hebergement.u-psud.fr/XPS/